Ingredients for use in personal care compositions

Inventors

Pereira, AbelBishop, ChristinaUzupis, Steven JezEdouard, FarahdiaDexter, MarniGunderman, Erik

Assignees

Croda Inc

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Publication Number

US-11478416-B2

Patent

Publication Date

2022-10-25

Expiration Date


Abstract

A dialkyl amidoamine which is the reaction product of a polyamine, a monocarboxylic acid, or a triglyceride or derivative thereof, and optionally an epoxide-containing compound is described. The dialkyl amidoamine may be used as a conditioning agent or anti-frizz agent useful in personal care applications, particularly in the conditioning of hair. The preparation and use of a conditioning agent and an anti-frizz agent comprising the dialkyl amidoamine are also described.

Core Innovation

The invention provides a conditioning agent comprising a dialkyl amidoamine that is the reaction product of a polyamine selected from diethylene triamine (DETA) and triethylene tetramine (TETA), a monocarboxylic acid selected from isostearic acid, oleic acid, palmitic acid, linoleic acid, or obtained from palm oil, rape seed oil or HEAR (high erucic acid rape) oil, and an epoxide-containing compound selected from ethylene oxide, propylene oxide and glycidol. The dialkyl amidoamine is defined by tertiary amine content >95% as determined using AOCS method Tf 3a-64 and is substantially free from quaternary ammonium compounds.

The conditioning agent is positioned for hair conditioning and includes formulations where the conditioning agent is used as a personal care ingredient. The document also describes delivery forms such as a predispersion or presolution that include the conditioning agent with a dispersing agent and/or a solvent.

In parallel, the invention provides an anti-frizz agent comprising the same class of dialkyl amidoamine reaction products, with the same polyamine selection, monocarboxylic acid selection, and epoxide-containing compound selection, and with the same tertiary amine content constraint (>95% using AOCS method Tf 3a-64). The anti-frizz agent is also defined as substantially free from quaternary ammonium compounds and is described with improved frizz control on hair relative to untreated hair based on wet/dry combing force and frizz control testing.

Claims Coverage

The document includes two independent claims: one directed to a conditioning agent and one directed to an anti-frizz agent. Across both independent claims, the inventive concept is implemented with three composition-defining elements together with a tertiary amine content requirement and a requirement of being substantially free from quaternary ammonium compounds.

Conditioning agent defined by dialkyl amidoamine reaction product composition and tertiary amine content

A conditioning agent comprising at least 50% by weight of a dialkyl amidoamine that is the reaction product of a polyamine selected from diethylene triamine (DETA) and triethylene tetramine (TETA), a monocarboxylic acid selected from isostearic acid, oleic acid, palmitic acid, linoleic acid or obtained from palm oil, rape seed oil or HEAR oil, and an epoxide-containing compound selected from ethylene oxide, propylene oxide and glycidol, wherein tertiary amine content of the dialkyl amidoamine is >95% as determined using AOCS method Tf 3a-64.

Conditioning agent substantially free from quaternary ammonium compounds

The conditioning agent is substantially free from quaternary ammonium compounds.

Anti-frizz agent defined by dialkyl amidoamine reaction product composition and tertiary amine content

An anti-frizz agent comprising a dialkyl amidoamine which is the reaction product of a polyamine selected from diethylene triamine (DETA) and triethylene tetramine (TETA), a monocarboxylic acid selected from isostearic acid, oleic acid, palmitic acid, linoleic acid or obtained from palm oil, rape seed oil or HEAR oil, and an epoxide-containing compound selected from ethylene oxide, propylene oxide and glycidol, wherein tertiary amine content of the dialkyl amidoamine is >95% as determined using AOCS method Tf 3a-64.

Anti-frizz agent substantially free from quaternary ammonium compounds

The anti-frizz agent is substantially free from quaternary ammonium compounds.

Overall, claim coverage centers on dialkyl amidoamine reaction products defined by specific polyamines, monocarboxylic acids, and epoxide-containing compounds, with tertiary amine content >95% by AOCS Tf 3a-64 and substantially no quaternary ammonium compounds. One independent claim specifies the composition as a conditioning agent, and the other specifies the composition as an anti-frizz agent.

Stated Advantages

Improved frizz resistance for treated hair, as indicated by frizz control testing and reported changes in wet/dry combing force.

Documented Applications

Conditioning formulations for hair, including use as a conditioning agent in personal care formulations.

Anti-frizz use for hair, including performance evaluation via frizz control testing and wet/dry combing force comparisons to untreated hair.

Use of the conditioning agent in predispersion or presolution comprising the conditioning agent together with a dispersing agent and/or a solvent.

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