Apparatus and method to identify and measure gas concentrations

Inventors

Uplinger, II, James RobertNICHOL, ROBERT MKeller, Walter John

Assignees

Nokomis Inc

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Publication Number

US-11229379-B2

Patent

Publication Date

2022-01-25

Expiration Date


Abstract

A method and apparatus is provided for the analysis of gaseous compounds, especially for determining the concentration of a gas or gases in a gas mixture by microwave spectroscopy. Microwave radiation is generated at one or more frequencies the gas is most responsive to, transmitted by antenna, passed through the gas under test, received by antenna, and the absorption and/or reflection of the microwave radiation is measured by means such as digitization and analysis using the FFT spectrum versus energy response generated, the response subsequently used to calculate the gas concentration.

Core Innovation

The invention provides a microwave/RF spectroscopy approach for non-contact gas concentration identification and quantification by passing a gas mixture through an electromagnetic field generated by a pair of antennas. The system measures one of an absorption amplitude, an emission amplitude, and a reflection amplitude of the gas mixture, or measures an electromagnetic energy difference between an emission spectrum transmitted from a transmit antenna and an emission spectrum absorbed or reflected by gaseous molecules. The measured values are converted to an absolute gas mixture concentration.

The converted absolute gas mixture concentration is compared against a stored value, and the gas mixture is analyzed based on a result of the comparison. In another configuration, the electromagnetic energy difference is converted into a digital signal, one of an absorption amplitude, an emission amplitude, a reflection amplitude, and any combinations thereof is measured in the digital signal, the measured amplitude is converted to an absolute concentration, and the absolute concentration is compared against a stored value.

The apparatus and handling configurations include a hollow enclosure and antenna arrangements that support measurement of microwave electromagnetic energy through the gas mixture while the gas mixture flows between a transmit antenna and a receive antenna. The hollow enclosure may be configured as a Faraday cage with the antennas encased therein, and the document also describes optional intake and evacuation members associated with the hollow enclosure. A control system digitizes the captured signals, processes the resulting spectrum or energy response, and performs comparison and analysis, including use with exhaled breath and medical-condition presence or absence.

Claims Coverage

The independent claims cover three method aspects: measuring absorption, emission, or reflection amplitudes and converting them to an absolute concentration for comparison-based analysis; conducting a controlled gas-flow experiment in a hollow enclosure, including evacuation and optionally Faraday shielding, to capture an electromagnetic energy difference and determine an absolute concentration for comparison; and determining concentration by transmitting and capturing an electromagnetic energy difference from absorption or reflection in a gas mixture with subsequent digital processing and analysis. Across these independent claims, at least seven main inventive features are recited in varying combinations.

Absorption, emission, or reflection amplitude measurement for absolute concentration

Measuring one of an absorption amplitude, an emission amplitude and a reflection amplitude of the gas mixture; converting the one of the absorption amplitude, the emission amplitude and the reflection amplitude to an absolute gas mixture concentration; comparing the absolute gas mixture concentration against a stored value; and analyzing the gas mixture based on a result of a comparison of the absolute gas mixture concentration against the stored value.

Pair of spaced antennas generating an electromagnetic field

Passing a gas mixture through an electromagnetic field generated by a pair of antennas being spaced apart with each other.

Electromagnetic energy difference capture for concentration determination

Capturing, with a receive antenna spaced from the transmit antenna so that the gas mixture flows between the transmit antenna and the receive antenna, an electromagnetic energy difference between an electromagnetic energy emission spectrum transmitted from the transmit antenna and an electromagnetic energy emission spectrum being absorbed or reflected by gaseous molecules in the gas mixture.

Digital signal conversion and amplitude measurement

Converting the electromagnetic energy difference into a digital signal; measuring in the digital signal, with a control member, one of an absorption amplitude, an emission amplitude, a reflection amplitude, and any combinations thereof.

Absolute concentration conversion and comparison to stored value

Converting the one of the absorption amplitude, the emission amplitude, the reflection amplitude, and any combinations thereof to an absolute concentration; and comparing, with the control member, the absolute concentration against a stored value.

Hollow enclosure intake and evacuation for controlled gas handling

Introducing, with an intake member attached to a hollow enclosure, a gas mixture into the hollow enclosure; evacuating, with an evacuation member attached to the hollow enclosure, the gas mixture from the hollow enclosure.

Faraday cage hollow enclosure encasing antennas

Providing the hollow enclosure as a Faraday cage and encasing the receive and transmit antennas within it.

Transmit antenna coupled to a microwave generator

Transmitting, with a transmit antenna coupled to a microwave generator, an electromagnetic energy emission spectrum through the gas mixture.

Determining concentration from analysis of electromagnetic energy difference

Determining, with a control member configured to process the digital signal, a concentration of gasses in the gas mixture based on an analysis of the electromagnetic energy difference.

Across the independent claims, the central claim coverage is directed to measuring absorption, emission, or reflection amplitudes or an electromagnetic energy difference produced by absorption or reflection of gaseous molecules, converting the resulting signal into absolute concentration via digital processing, and using that concentration for comparison-based analysis, including comparison against stored values, with independent claim variants covering antenna spacing, hollow-enclosure intake and evacuation, and optional Faraday cage encasing.

Stated Advantages

Sensitivity enabling low microwave transmit power.

SAR-limited exposure.

Documented Applications

Analyzing expirate/breath to determine presence or absence of a medical condition in a person.

Determining whether a presence or absence or a medical condition exists in the person based on the analyzing of the expirate.

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